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Thus, the Ti decreases drastically in the whole process of heating since the nitrogen oxide and vapor are very easily released accompanying the thermal decomposition of nitrogen-containing compounds at low temperatures [21], that's confirmed by the TG-IR final results. Moreover, it can be worth noting that FR-PA66 demonstrates two decomposition peaks compared with pure PA66, as well as the Tmax2 is larger than the Tmax1 of pure PA66 regardless of the material of HCNP. This phenomenon can be due to the dehydration response of CNHO teams as well as the dehydrogenation response of α-CH2 facilitated via the R-P· free of charge radical substances manufactured from HCNP, accelerating the formation on the protecting compact char levels [22].
Then again, the stable multilayer carbonaceous chars (Determine five) produced from the response amongst HCNP as well as decomposition goods of PA66 can insulate the underlying substrate from your warmth source and slow down equally the heat and mass transfer [25]. As a result, it can be summarized that HCNP can efficiently Increase the flame retardancy of PA66 adhering to the gasoline-period flame retardant system.
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PA66 pellets and HCNP powder were dried for 4 h at a hundred °C ahead of extrusion. The FR-PA66 was organized by twin-screw extrusion response in the number of 260–270 °C. The take a look at samples were manufactured employing a TTI-95G injection molding machine underneath 265 °C using a 180 r/min rotation pace. Determine six reveals the microtopography of pure PA66, HCNP, and FR-PA66. It may be noticed from Figure 6c that the HCNP microspheres have been dispersed a lot more uniformly with out noticeable section interfaces, along with the peeling phenomenon appeared around the area with the microspheres (Determine 6d), indicating that the terminal carboxyl groups of PA66 ended up chemically bonded Using the amino groups around the surface area of your microspheres over the extrusion reaction, which ruined the regularity of the floor in the microspheres (Determine 6b, sleek surface area and no peeling phenomenon) and led towards the core–shell separation with the microspheres (Determine 6d), confirming the prevalence on the in situ loading reaction.